Evaluation of nanomanganese decorated typha tassel carbonaceous electrode: preparation, characterization, and simultaneous determination of Cd2+ and Pb2+

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dc.contributor.authorGüleşen, Mustafa
dc.contributor.authorErkal-Aytemur, Aslı
dc.contributor.authorYavuz, Samet
dc.contributor.authorAkbulut, Abdullah
dc.contributor.authorKariper, I. Afşin
dc.contributor.authorÜstündağ, İlknur
dc.date.accessioned2021-02-19T21:16:16Z
dc.date.available2021-02-19T21:16:16Z
dc.date.issued2019
dc.departmentALKÜ
dc.descriptionUstundag, Ilknur/0000-0002-9557-3658; AKBULUT, ABDULLAH/0000-0002-6199-4083
dc.description.abstractIn this study, manganese dioxide decorated typha tassel carbonized material was prepared. The pyrolysis of the carbonaceous material occurred in a tube furnace at 800 degrees C under nitrogen atmosphere. MnO2 nanoparticles on typha tassel (CT) were synthesized with sol-gel method. The final product was denoted as MTT electrode (MnO2-CT). The carbonaceous material was characterized with infrared spectroscopy, X-ray photoelectron spectroscopy, scanning electron microscopy and X-ray diffraction methods. Electrode usability performance of the material was examined via electrochemical techniques. An electrochemical method was developed with stripping voltammetry for the analysis of heavy metals such as Pb2+ and Cd2+ on the MCT electrode. The linear equations for Cd2+ and Pb2+ were computed. The limit of detection (S/N = 3) was 0.05 mu g/L for Cd2+ and 0.01 mu g/L for Pb2+ within the range of 0.5-50 mu g/L and 0.2-50 mu g/L, respectively. The method was successfully applied to the simultaneous determination of Cd2+ and Pb2+ in tap water and milk samples.
dc.identifier.doi10.1007/s11696-019-00839-1
dc.identifier.endpage2878en_US
dc.identifier.issn2585-7290
dc.identifier.issn1336-9075
dc.identifier.issue11en_US
dc.identifier.scopusqualityQ2
dc.identifier.startpage2869en_US
dc.identifier.urihttps://doi.org/10.1007/s11696-019-00839-1
dc.identifier.urihttps://hdl.handle.net/20.500.12868/356
dc.identifier.volume73en_US
dc.identifier.wosWOS:000482434100023
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthor0-belirlenecek
dc.language.isoen
dc.publisherSpringer International Publishing Ag
dc.relation.ispartofChemical Papers
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCarbonaceous material
dc.subjectMnO2 decorated typha tassel
dc.subjectElectrode material
dc.subjectDifferential pulse anodic stripping voltammetry
dc.titleEvaluation of nanomanganese decorated typha tassel carbonaceous electrode: preparation, characterization, and simultaneous determination of Cd2+ and Pb2+
dc.typeArticle

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