Validation of Quick Polar Pesticides (QuPPe) Method for Determination of Eight Polar Pesticides in Cherries by LC-MS/MS

Basit Öğe Kaydı
dc.authorid0000-0001-5020-339X
dc.contributor.authorGolge, Ozgur
dc.date.accessioned2026-01-24T12:31:01Z
dc.date.available2026-01-24T12:31:01Z
dc.date.issued2021
dc.departmentAlanya Alaaddin Keykubat Üniversitesi
dc.description.abstractA novel and sensitive chromatography method with modified Quick Polar Pesticide (QuPPe) sample preparation was validated for determination of eight high polar pesticides in cherries by liquid chromatography-triple quadrupole mass spectrometry (LC-MS/MS). The validation data executed the conditions of the European SANTE/12682/2019 Guidance Document. Good linearity (R-2 > 0.99) was observed, and the residuals were lower than +/- 20%. Average recoveries ranged from 70.2 to 105.1%, and LOQ values ranged from 1.77 to 12.13 mu g kg(-1). The repeatability and reproducibility are in range of 1.57-15.56% and 3.51-16.17% separately. All measurement uncertainty values were lower than 50% for all polar pesticides. This verified analytical method was used to detect pesticide residue levels of cherries, and none of the eight high polar pesticides were found in 225 real samples. This is the first validation report of QuPPe sample preparation and LC-MS/MS method of high polar pesticide residues in cherries from Turkey.
dc.identifier.doi10.1007/s12161-021-01966-w
dc.identifier.endpage1437
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue7
dc.identifier.scopus2-s2.0-85101725317
dc.identifier.scopusqualityQ1
dc.identifier.startpage1432
dc.identifier.urihttps://doi.org/10.1007/s12161-021-01966-w
dc.identifier.urihttps://hdl.handle.net/20.500.12868/5593
dc.identifier.volume14
dc.identifier.wosWOS:000620433800001
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofFood Analytical Methods
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20260121
dc.subjectHigh polar pesticides
dc.subjectLC-MS
dc.subjectMS
dc.subjectMethod validation
dc.subjectQuPPe
dc.subjectCherries
dc.titleValidation of Quick Polar Pesticides (QuPPe) Method for Determination of Eight Polar Pesticides in Cherries by LC-MS/MS
dc.typeArticle

Dosyalar

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu