Determination of more than 500 Pesticide Residues in Hen Eggs by Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) and Gas Chromatography-Tandem Mass Spectrometry (GC/MS/MS)

dc.contributor.authorGölge, Özgür
dc.contributor.authorLiman, Turan
dc.contributor.authorKabak, Bülent
dc.date.accessioned2022-09-23T08:33:45Z
dc.date.available2022-09-23T08:33:45Z
dc.date.issued2021
dc.departmentALKÜ, Fakülteler, Turizm Fakültesi, Gastronomi ve Mutfak Sanatları Bölümü
dc.description.abstractThis study aims to validate a fast method of simultaneous analysis of 365 LC-amenable and 142 GC-amenable pesticides in hen eggs by liquid chromatography-tandem mass spectrometry (LC-MS/MS) and gas chromatography-tandem mass spectrometry (GC-MS/MS), respectively, operating in multiple reaction monitoring (MRM) acquisition modes. The sample preparation was based on quick, easy, cheap, effective, rugged, and safe (QuEChERS) extraction. Key method performance parameters investigated were specificity, linearity, limit of quantification (LOQ), accuracy, precision and measurement uncertainty. The method was validated at two spiking levels (10 and 50 mu g/kg), and good recoveries (70%-120%) and relative standard deviations (RSDs) (<= 20) were achieved for 92.9% of LC-amenable and 86.6% of GC-amenable pesticide residues. The LOQs were <= 10 mu g/kg for 94.2% of LC-amenable and 92.3% of GC-amenable pesticides. The validated method was further applied to 100 egg samples from caged hens, and none of the pesticides was quantified.
dc.identifier.doi10.5851/kosfa.2021.e38
dc.identifier.endpage825en_US
dc.identifier.issue5en_US
dc.identifier.startpage816en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12868/1664
dc.identifier.urihttps://www.kosfaj.org/archive/view_article?pid=kosfa-41-5-816
dc.identifier.volume41en_US
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.language.isoen
dc.relation.ispartofFood Science of Animal Resources
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectPesticides
dc.subjectHen eggs
dc.subjectFood safety
dc.subjectMonitoring
dc.subjectMethod validation
dc.titleDetermination of more than 500 Pesticide Residues in Hen Eggs by Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) and Gas Chromatography-Tandem Mass Spectrometry (GC/MS/MS)
dc.typeArticle

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Yükleniyor...
Küçük Resim
İsim:
kosfa-41-5-816.pdf
Boyut:
485.6 KB
Biçim:
Adobe Portable Document Format
Açıklama:
Tam metin / Full Text
Lisans paketi
Listeleniyor 1 - 1 / 1
[ X ]
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama: