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    Characterizing damage evolution of CF/PEKK composites under tensile loading through multi-instrument structural health monitoring techniques
    (Elsevier Sci Ltd, 2023) Yildirim, Ceren; Tabrizi, Isa Emami; Al-Nadhari, Abdulrahman; Topal, Serra; Beylergil, Bertan; Yildiz, Mehmet
    This study investigates the damage behavior of autoclave consolidated carbon fiber/Polyetherketoneketone (CF/ PEKK) laminates manufactured by the automated fiber placement (AFP) lay-up process. The damage evaluation of autoclave consolidated samples is studied using a multi-instrument nondestructive monitoring approach. The effect of autoclave consolidation on the microstructure of the laminate is examined via void analysis based on density measurement, thermal analysis, and optical microscopy. The results reveal that the void content is achieved as 0.46% and there is 81.81% increase in the degree of crystallinity following the autoclave consolidation. Moreover, acoustic emission (AE), digital image correlation (DIC), and infrared thermography (IRT) results are cross-correlated to further understand the damage development. The evolution of clustered AE data during mechanical loading is used to divide the failure of the laminate into two stages, each of which signifies a different dominancy in failure modes. Scanning electron microscopy (SEM) is employed to associate damage characteristics with failure monitoring techniques.
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    Öğe
    Effect of atmospheric plasma treatment on Mode-I and Mode-II fracture toughness properties of adhesively bonded carbon fiber/PEKK composite joints
    (Pergamon-Elsevier Science Ltd, 2023) Yildirim, Ceren; Ulus, Hasan; Beylergil, Bertan; Al-Nadhari, Abdulrahman; Topal, Serra; Yildiz, Mehmet
    This study aims to assess the influence of peel-ply (PP), mechanical abrasion (MA), and atmospheric plasma activation (APA) treatments on Mode-I and Mode-II fracture toughness of carbon fiber/ poly-ether-ketone-ketone (CF/PEKK) composite joints. A comprehensive examination of the topography and wettability of the adherend surfaces is conducted using various methods. The CF/PEKK adherends are produced through an automated fiber placement (AFP) process, and the CF/PEKK bonded joints are prepared using two different structural adhesive films, one of which has a lower strength, while the other has a higher strength. To evaluate their fracture toughness properties, double cantilever beam (DCB) and end-notched flexure (ENF) tests are carried out in accordance with ASTM standards. Acoustic emission sensors are used to monitor the test specimens during DCB tests, allowing for an in-depth evaluation of the failure modes and damage propagations in the joints. The results show that the GIC and GIIC values of the APA-treated CF/ PEKK bonded joints are remarkably higher than those of the untreated ones, with a range of improvement of 34.0-84.8 times and 7.5-17.4 times, respectively. Adhesive failure is the dominant failure mode on the surfaces of non-treated (NT) and PP samples, while cohesive failure is more prominent in those treated with MA and APA. The failure modes of the treated samples varied depending on the adhesive used, with APA-treated samples always exhibiting a cohesive failure. It is observed that the AE counts increase more slowly in APA-treated samples compared to MA-treated joints as delamination progresses more slowly with cohesive failure dominant, which leads to a lower release of AE energy.
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    Öğe
    Tailoring adherend surfaces for enhanced bonding in CF/PEKK composites: Comparative analysis of atmospheric plasma activation and conventional treatments
    (Elsevier Sci Ltd, 2024) Yildirim, Ceren; Ulus, Hasan; Beylergil, Bertan; Al-Nadhari, Abdulrahman; Topal, Serra; Yildiz, Mehmet
    Here, we propose the utilization of atmospheric plasma activation (APA), which outperforms peel-ply (PP) treatment and mechanical abrasion (MA) in achieving high-performance adhesively bonded carbon fiber/polyetherketoneketone (CF/PEKK) composites. This study covers several key aspects, including the chemical and morphological characterization of treated surfaces and mechanical performance assessments of single lap-joints (SLJs) under tensile and flexural loading conditions. In addition, in-situ acoustic emission (AE) monitoring is employed during tensile tests to determine dominant damage types and failure modes in the SLJs. Surface analysis shows that MA increases roughness, PP treatment decreases wettability, while APA enhances wettability by modifying the surface chemistry. Tensile and flexural tests reveal that APA-treated joints surpassed nontreated (NT) ones, with up to 5- and 7-times higher load-carrying performance, respectively, while fracture analysis suggests a shift from adhesive to cohesive failure. AE results show that increased AE events related to cohesive failure align with improved interface interactions.